3-sydnone

Base Information

Chemical Name:3-sydnone
CAS No.:103248-65-3
Molecular Formula:C₁₁H₈N₄O₂
Molecular Weight:228.21
Hs Code.:

Synonyms:

Suppliers and Price of 3-sydnone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-sydnone

Chemical Property:

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Technology Process of 3-sydnone

There total 4 articles about 3-sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 78786-56-8
N-Nitroso-N-phenylglycine

: 103248-65-3
3-sydnone

Guidance literature:: With acetic anhydride; for 3h;
DOI:10.1002/ardp.19813140605

Reference yield:

: (2-Pyrazol-1-yl-phenylamino)-acetic acid ethyl ester

: 103248-65-3
3-sydnone

Guidance literature:: Multi-step reaction with 3 steps

1: 10 percent aq. NaOH / ethanol

2: NaNO₂, 25 percent aq. HCl / 3 h

3: 61 percent / acetic anhydride / 3 h

With hydrogenchloride; sodium hydroxide; acetic anhydride; sodium nitrite; In ethanol;
DOI:10.1002/ardp.19813140605

Reference yield:

: 54705-91-8
2-(1H-pyrazol-1-yl)aniline

: 103248-65-3
3-sydnone

Guidance literature:: Multi-step reaction with 4 steps

1: aq. sodium acetate / ethanol / 40 h / 130 °C

2: 10 percent aq. NaOH / ethanol

3: NaNO₂, 25 percent aq. HCl / 3 h

4: 61 percent / acetic anhydride / 3 h

With hydrogenchloride; sodium hydroxide; sodium acetate; acetic anhydride; sodium nitrite; In ethanol;
DOI:10.1002/ardp.19813140605