(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

Base Information

Chemical Name:(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃
CAS No.:94365-52-3
Molecular Formula:C₃₄H₃₁CuN₅P
Molecular Weight:604.173
Hs Code.:

(PPh<sub>3</sub>)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN<sub>3</sub>

Synonyms:

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Chemical Property of (PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

Chemical Property:

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Technology Process of (PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

There total 1 articles about (PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1660-93-1
3,4,7,8-Tetramethyl-o-phenanthrolin

: azidobis(triphenylphosphine)copper(I)

: 94365-52-3
(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

Guidance literature:: In dichloromethane; addn. of N2C12H4Me4 to soln. of ((PPh3)2CuN3)2 (ligand:Cu ratio = 1.1) with stirring;; evapg. to dryness after 1 h; treating residue several times with toluene; filtering, washing with n-hexane and drying; elem. anal.;;
DOI:10.1016/0022-328X(84)80531-8

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 94365-52-3
(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

: 94365-54-5
(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)Cu(NC(S)SN₂)

Guidance literature:: With triphenylphosphine; In benzene; addn. of (PPh3)(N2CC12H4Me4)CuN3 (0.3 mmol) to benzene soln. contg. PPh3 (0.38 mmol) and freshly distd. CS2 (3.3 mmol); stirring suspension in the dark for 6 h (react. is monitored by IR);; filtering, washing with benzene and n-hexane and drying in vac.; elem. anal.;;
DOI:10.1016/0022-328X(84)80531-8

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 94365-52-3
(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)CuN₃

: 94365-56-7
(PPh₃)(3,4,7,8-tetramethyl-1,10-phenanthroline)Cu(NCS)

Guidance literature:: In benzene; addn. of (PPh3)(N2CC12H4Me4)CuN3 to benzene soln. contg. freshly distd.CS2; stirring suspension in the dark for 6 h (react. is monitored by IR);; filtering, washing with benzene and n-hexane and drying in vac.; elem. anal.;;
DOI:10.1016/0022-328X(84)80531-8