CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

Base Information

Chemical Name:CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2
CAS No.:203799-89-7
Molecular Formula:C₁₉H₂₀CrN₂O₅
Molecular Weight:408.374
Hs Code.:

CH<sub>2</sub>CHC<sub>2</sub>H<sub>4</sub>C[Cr(CO)5]N(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)N(CH<sub>3</sub>)2

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Suppliers and Price of CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

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Technology Process of CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

There total 2 articles about CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-pentacarbonyl[(N-benzyl-N',N''-dimethylhydrazinyl)methyl carbene]chromium⁽⁰⁾

: 106-95-6
allyl bromide

: 203799-90-0
CH₂CHC₂H₄C[Cr(CO)4]N(CH₂C₆H₅)N(CH₃)2

: 203799-89-7
CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

Guidance literature:: With nBuLi; In tetrahydrofuran; (N2); react. of complex with BuLi at -78°C for 30 min, addn. of bromide, react. at -78°C for 10 min and at 0°C for 30 min; column chromy.;
DOI:10.1039/a708018b

Reference yield:

: disodium pentacarbonylchromium

: 78817-44-4
acetic acid N-benzyl-N',N'-dimethyl-hydrazide

: 203799-90-0
CH₂CHC₂H₄C[Cr(CO)4]N(CH₂C₆H₅)N(CH₃)2

: 203799-89-7
CH₂CHC₂H₄C[Cr(CO)5]N(CH₂C₆H₅)N(CH₃)2

Guidance literature:: Multi-step reaction with 2 steps

1: (CH₃)3SiCl / tetrahydrofuran

2: nBuLi / tetrahydrofuran

With (CH₃)3SiCl; nBuLi; In tetrahydrofuran;
DOI:10.1039/a708018b