10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one

Base Information

Chemical Name:10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one
CAS No.:37439-92-2
Molecular Formula:C₂₀H₁₉NO
Molecular Weight:289.377
Hs Code.:
European Community (EC) Number:609-429-3
DSSTox Substance ID:DTXSID101221446

Synonyms:10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one;SCHEMBL9904943;KIPXMFZJKGQNDR-UHFFFAOYSA-N;DTXSID101221446;37439-92-2;10-(1-piperidyl)-5H-dibenzo[a,d]cyclohepten-5-one

Suppliers and Price of 10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C
XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:289.146664230
Heavy Atom Count:22
Complexity:449

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCN(CC1)C2=CC3=CC=CC=C3C(=O)C4=CC=CC=C42

Technology Process of 10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one

There total 4 articles about 10-(1-piperidinyl)-5H-dibenzo[a,d]cyclohepten-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 110-89-4
piperidine

: 17044-50-7
10-bromo-5H-dibenzo[a,d]cyclohepten-5-one

: 37439-92-2
10-piperidin-1-yl-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 20 - 85 ℃; Inert atmosphere;

Reference yield:

: 2222-33-5
dibenzosuberenon

: 37439-92-2
10-piperidin-1-yl-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / tetrachloromethane / 5.25 h

2: sodium hydroxide / methanol / 6 h / 70 °C / Inert atmosphere

3: potassium tert-butylate / tert-butyl alcohol / 20 - 85 °C / Inert atmosphere

With potassium tert-butylate; bromine; sodium hydroxide; In methanol; tetrachloromethane; tert-butyl alcohol;

Reference yield:

: 57295-97-3
10,11-dibromo[(10,11-dihydro-5H-dibenzo[a,d]cyclohept-5-one)]

: 37439-92-2
10-piperidin-1-yl-dibenzo[a,d]cyclohepten-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol / 6 h / 70 °C / Inert atmosphere

2: potassium tert-butylate / tert-butyl alcohol / 20 - 85 °C / Inert atmosphere

With potassium tert-butylate; sodium hydroxide; In methanol; tert-butyl alcohol;