2-amino-4-methyl-3,5-dinitro-benzophenone

Base Information

• Chemical Name: 2-amino-4-methyl-3,5-dinitro-benzophenone
• CAS No.: 854020-49-8
• Molecular Formula: C₁₄H₁₁N₃O₅
• Molecular Weight: 301.258
• Mol file: 854020-49-8.mol

Synonyms:

Chemical Property of 2-amino-4-methyl-3,5-dinitro-benzophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-amino-4-methyl-3,5-dinitro-benzophenone

There total 2 articles about 2-amino-4-methyl-3,5-dinitro-benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4-methyl-3,5-dinitro-benzophenone → 2-amino-4-methyl-3,5-dinitro-benzophenone (854020-49-8)

Guidance literature:

With ammonia; at 150 ℃;

DOI:10.1002/hlca.660280182

Reference yield:

2-chloro-4-methyl-3,5-dinitro-benzoic acid (200265-71-0) → 2-amino-4-methyl-3,5-dinitro-benzophenone (854020-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅; benzene / 4-taegiges Behandeln des erhaltenen Saeurechlorids mit Benzol und AlCl₃

2: ethanolic ammonia / 150 °C

With phosphorus pentachloride; ammonia; benzene;

DOI:10.1002/hlca.660280182

Reference yield:

2-amino-4-methyl-3,5-dinitro-benzophenone (854020-49-8) → 3-methyl-2,4-dinitro-fluoren-9-one (70621-46-4)

Guidance literature:

With sulfuric acid; sodium nitrite; at 20 ℃; anschliessendes Erhitzen auf 110-120grad;

DOI:10.1002/hlca.19490320716

upstream raw materials:

2-chloro-4-methyl-3,5-dinitro-benzoic acid

Downstream raw materials:

3-methyl-2,4-dinitro-fluoren-9-one