5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

Base Information

Chemical Name:5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester
CAS No.:129168-50-9
Molecular Formula:C₃₂H₃₀N₄O₄
Molecular Weight:534.615
Hs Code.:

5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenz<c>azocin-6-carbonsaeuremethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

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Technology Process of 5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

There total 2 articles about 5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 129168-46-3,129214-65-9
5-Hydroxy-5-methyl-3t,11anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

: 103-71-9
phenyl isocyanate

: 129168-50-9
5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

Guidance literature:: In tetrahydrofuran; for 5h; Heating;
DOI:10.1002/ardp.19903230309

Reference yield:

: 42906-87-6,106975-24-0,119718-14-8,121156-18-1
5-Oxo-3t,11anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethyl-ester

: 129168-50-9
5t-Methyl-5c-N-phenylcarbamoyl-3t,11-anti-di-2-pyridyl-4,5-dihydro-1H,3H-2r,6c-methanobenzazocin-6-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.25 h / ice cooling

2: 60 percent / tetrahydrofuran / 5 h / Heating

In tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.19903230309