(3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one

Base Information

• Chemical Name: (3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one
• CAS No.: 98380-60-0
• Molecular Formula: C₄₁H₄₅N₃O₅
• Molecular Weight: 659.825

Synonyms:

Chemical Property of (3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one

Chemical Property:

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Safty Information:

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Useful:

Technology Process of (3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one

There total 12 articles about (3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(3R,4S)-1-<(S)-1-(hydroxycarbonyl)ethyl>-3-(benzyloxy)-4-phenylazetidin-2-one (98380-68-8) + (3S,4R)-3-Amino-1-((S)-1-benzyloxymethyl-3-methyl-butyl)-4-phenyl-azetidin-2-one (82101-50-6) → (3S,4R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one (98380-60-0,98463-75-3,136778-98-8)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00018a012

Reference yield: 81.0%

(3R,4S)-3-Amino-1-((S)-1-benzyloxymethyl-3-methyl-butyl)-4-phenyl-azetidin-2-one (98463-78-6) + (3R,4S)-1-<(S)-1-(hydroxycarbonyl)ethyl>-3-(benzyloxy)-4-phenylazetidin-2-one (98380-68-8) → (3R,4S)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<(S)-2-<(3'R,4'S)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>-4-phenylazetidin-2-one (98380-60-0,98463-75-3,136778-98-8)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00018a012

Reference yield: 68.0%

(3R,4S)-3-Amino-1-((S)-1-benzyloxymethyl-3-methyl-butyl)-4-phenyl-azetidin-2-one (98463-78-6) + (3S,4R)-1-<(S)-1-(hydroxycarbonyl)ethyl>-3-(benzyloxy)-4-phenylazetidin-2-one (98463-81-1) → (3R,4S)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-3-<<(S)-2-<(3'S,4'R)-3'-(benzyloxy)-2'-oxo-4'-phenylazetidin-1'-yl>propanoyl>amino>-4-phenylazetidin-2-one (98380-60-0,98463-75-3,136778-98-8)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00018a012

upstream raw materials:

(3R,4S)-3-Amino-1-((S)-1-benzyloxymethyl-3-methyl-butyl)-4-phenyl-azetidin-2-one

(3S,4R)-1-<(S)-1-(hydroxycarbonyl)ethyl>-3-(benzyloxy)-4-phenylazetidin-2-one

Benzyloxyacetyl chloride

(S)-N-benzylidene-1-t-butoxycarbonylethylamine

Downstream raw materials:

[(2S,3S)-1-((S)-1-Benzyloxymethyl-3-methyl-butyl)-2-phenyl-azetidin-3-yl]-[(S)-2-((2R,3R)-3-benzyloxy-2-phenyl-azetidin-1-yl)-propyl]-amine

[(2S,3S)-1-((S)-1-Benzyloxymethyl-3-methyl-butyl)-2-phenyl-azetidin-3-yl]-[(S)-2-((2S,3S)-3-benzyloxy-2-phenyl-azetidin-1-yl)-propyl]-amine

(2R,5S,8S,11S)-2,8-dibenzyl-5,13-dimethyl-11-(hydroxymethyl)-1-oxa-4,7,10-triazatetradecane

(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-<<(S)-2-<(2'S,3'S)-2'-phenyl-3'-(benzyloxy)azetidin-1-yl>propyl>amino>azetidine

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