2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

Base Information

Chemical Name:2'-deoxycytidine cyclic 3'-5'-phosphoranilidate
CAS No.:90662-79-6
Molecular Formula:C₁₅H₁₇N₄O₅P
Molecular Weight:364.298
Hs Code.:

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Chemical Property of 2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

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Technology Process of 2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

There total 2 articles about 2'-deoxycytidine cyclic 3'-5'-phosphoranilidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90662-54-7
5'-O-monomethoxytrityl-2'-deoxycytidine 3'-O-(2-chlorophenyl) phosphoranilidate

: 90662-79-6
2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 2 percent toluene-p-sulphonic acid monohydrate / CHCl₃; methanol / 0.17 h / Ambient temperature

2: 45 percent / t-BuOK / N,N-dimethyl-acetamide / 20 h / Ambient temperature

With potassium tert-butylate; toluene-4-sulfonic acid; In methanol; chloroform; N,N-dimethyl acetamide;
DOI:10.1016/0040-4020(84)85099-1

Reference yield:

: 90662-72-9,90662-73-0
2'-deoxycytidine 3'-(2-chlorophenyl) phosphoranilidate

: 90662-79-6
2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

: 90662-78-5
2'-deoxycytidine cyclic 3'-5'-phosphoranilidate

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl acetamide; for 20h; Ambient temperature;
DOI:10.1016/0040-4020(84)85099-1