C₁₁⁽¹³⁾CH₁₈O

Base Information

Chemical Name:C₁₁⁽¹³⁾CH₁₈O
CAS No.:99302-14-4
Molecular Formula:C₁₂H₁₈O
Molecular Weight:179.263
Hs Code.:

C<sub>11</sub><sup>(13)</sup>CH<sub>18</sub>O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁⁽¹³⁾CH₁₈O

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Technology Process of C₁₁⁽¹³⁾CH₁₈O

There total 1 articles about C₁₁⁽¹³⁾CH₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99302-10-0,99302-11-1
C₁₁⁽¹³⁾CH₁₇N

: 99302-14-4
C₁₁⁽¹³⁾CH₁₈O

Guidance literature:: With water; silica gel; diisobutylaluminium hydride; Multistep reaction; 1.) hexane-pet.ether, -60 deg C, -20 deg C 1 h; 2.) hexane-pet.ether, rt 1h;

Reference yield:

: 99302-14-4
C₁₁⁽¹³⁾CH₁₈O

: 99302-28-0
retinonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether / 1 h / Heating

2: manganese dioxide / hexane / Ambient temperature

3: 1.) sodium hydride / 1.) THF, 30 min, rt; 2.) THF, 0 deg C, rt 2 h

4: 1.) diisobutylaluminium hydride; 2.) water/silicagel / 1.) hexane-pet.ether, -60 deg C, -20 deg C 1 h; 2.) hexane-pet.ether, rt 1h

5: 1.) sodium hydride / 1.) THF, 30 min, rt; 2.) THF, 0 deg C, rt 2 h

With manganese(IV) oxide; water; silica gel; sodium hydride; diisobutylaluminium hydride; In diethyl ether; hexane;

Reference yield:

: 99302-14-4
C₁₁⁽¹³⁾CH₁₈O

: 99302-18-8
C₁₂⁽¹³⁾CH₂₀O

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1 h / Heating

2: manganese dioxide / hexane / Ambient temperature

With manganese(IV) oxide; In diethyl ether; hexane;