7-O-Acetyl Ursodeoxycholic Acid Methyl Ester

Base Information

Chemical Name:7-O-Acetyl Ursodeoxycholic Acid Methyl Ester
CAS No.:75672-24-1
Molecular Formula:C₂₇H₄₄O₅
Molecular Weight:448.643
Hs Code.:
Mol file:75672-24-1.mol

Synonyms:

Suppliers and Price of 7-O-Acetyl Ursodeoxycholic Acid Methyl Ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
7-O-AcetylUrsodeoxycholicAcidMethylEster
500mg
$ 1190.00

Medical Isotopes, Inc.
7-O-AcetylUrsodeoxycholicAcidMethylEster
50 mg
$ 650.00

Total 3 raw suppliers

Chemical Property of 7-O-Acetyl Ursodeoxycholic Acid Methyl Ester

Chemical Property:

Melting Point:53-61°C
Boiling Point:518.9±25.0 °C(Predicted)
PKA:14.97±0.70(Predicted)
Density:1.10±0.1 g/cm3(Predicted)
Storage Temp.:Refrigerator, Under Inert Atmosphere
Solubility.:Dichloromethane, Methanol

Purity/Quality:

99% ^*data from raw suppliers

7-O-AcetylUrsodeoxycholicAcidMethylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 7-O-Acetyl Ursodeoxycholic Acid Methyl Ester is a reactant used in the preparation of bile acids and 3β-Ursodeoxycholic Acid.

Technology Process of 7-O-Acetyl Ursodeoxycholic Acid Methyl Ester

There total 8 articles about 7-O-Acetyl Ursodeoxycholic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 60384-30-7
methyl 3α,7β-diacetoxy-5β-cholan-24-oate

: 75672-24-1
methyl ursodeoxycholate 7-acetate

Guidance literature:: With methanol; sodium hydroxide; at 20 ℃; for 0.5h;

Reference yield:

: 10538-55-3
3α,7β-dihydroxy-5β-cholan-24-oic acid methyl ester

: 75672-24-1
methyl ursodeoxycholate 7-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / pyridine / 6 h / 20 °C

2: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; dmap; In pyridine; methanol;
DOI:10.1016/j.cclet.2014.04.001

Reference yield:

: 128-13-2
ursodeoxycholic acid

: 75672-24-1
methyl ursodeoxycholate 7-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 3 h / 50 °C

2: dmap; pyridine / dichloromethane / 2 h / 20 °C

3: sodium hydroxide; methanol / 0.5 h / 20 °C

With pyridine; methanol; dmap; sulfuric acid; sodium hydroxide; In dichloromethane;