triphenylphosphorane

Base Information

Chemical Name:triphenylphosphorane
CAS No.:110637-81-5
Molecular Formula:C₂₅H₂₇N₂PS₄
Molecular Weight:514.741
Hs Code.:

<bis(dimethyldithiocarbamyl)methylene>triphenylphosphorane

Synonyms:

Suppliers and Price of triphenylphosphorane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylphosphorane

Chemical Property:

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Technology Process of triphenylphosphorane

There total 5 articles about triphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.2%

: 137-26-8,93196-73-7
Thiram

: 110637-62-2
Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; iodide

: 110637-81-5
triphenylphosphorane

Guidance literature:: In 1,2-dimethoxyethane; for 1.5h; Heating;
DOI:10.1021/jo00233a008

Reference yield:

: 5293-84-5
chloromethyltriphenylphosphonium chloride

: 110637-81-5
triphenylphosphorane

Guidance literature:: Multi-step reaction with 3 steps

1: 86.2 percent / CHCl₃ / 8 h / Ambient temperature

2: 100 percent / NaI / CHCl₃ / 3 h / Ambient temperature

3: 56.2 percent / 1,2-dimethoxy-ethane / 1.5 h / Heating

With sodium iodide; In 1,2-dimethoxyethane; chloroform;
DOI:10.1021/jo00233a008

Reference yield:

: 110637-73-5
Benzyltriphenylphosphonium dimethyldithiocarbamate

: 110637-81-5
triphenylphosphorane

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / 1,2-dimethoxy-ethane / 2.5 h / Ambient temperature

2: 100 percent / NaI / CHCl₃ / 3 h / Ambient temperature

3: 56.2 percent / 1,2-dimethoxy-ethane / 1.5 h / Heating

With sodium iodide; In 1,2-dimethoxyethane; chloroform;
DOI:10.1021/jo00233a008