Technology Process of C3(13)C6H9FOS2
There total 1 articles about C3(13)C6H9FOS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-fluoro(13C6)aniline;
With
sodium nitrite;
In
sulfuric acid; water;
at 0 ℃;
for 2h;
potassium ethyl xanthogenate;
With
borax; sodium tetraborate decahydrate;
In
sulfuric acid; water;
at 20 - 72 ℃;
for 2h;
Further stages.;
DOI:10.1002/jlcr.1183
- Guidance literature:
-
Multi-step reaction with 3 steps
1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C
2: 86 percent / lithium hydroxide / acetonitrile; tetrahydrofuran; H2O / 19 h
With
lithium hydroxide; dihydrogen peroxide; urea; trifluoroacetic anhydride;
In
tetrahydrofuran; water; ethyl acetate; acetonitrile;
DOI:10.1002/jlcr.1183
- Guidance literature:
-
Multi-step reaction with 4 steps
1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C
2: 86 percent / lithium hydroxide / acetonitrile; tetrahydrofuran; H2O / 19 h
3: 72 percent / N-methylmorpholine / acetonitrile / 0.17 h
With
4-methyl-morpholine; lithium hydroxide; dihydrogen peroxide; urea; trifluoroacetic anhydride;
In
tetrahydrofuran; water; ethyl acetate; acetonitrile;
DOI:10.1002/jlcr.1183
