Technology Process of C12H13BrN2OSSe
There total 3 articles about C12H13BrN2OSSe which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride
2: Burgess Reagent / dichloromethane / 1.5 h / 50 °C
3: selenium; triethylamine / tetrahydrofuran / 1 h / Reflux
4: triethylamine / tetrahydrofuran / 3 h / Reflux
With
selenium; thionyl chloride; Burgess Reagent; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/psc.1276
- Guidance literature:
-
Multi-step reaction with 2 steps
1: selenium; triethylamine / tetrahydrofuran / 1 h / Reflux
2: triethylamine / tetrahydrofuran / 3 h / Reflux
With
selenium; triethylamine;
In
tetrahydrofuran;
DOI:10.1002/psc.1276
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Burgess Reagent / dichloromethane / 1.5 h / 50 °C
2: selenium; triethylamine / tetrahydrofuran / 1 h / Reflux
3: triethylamine / tetrahydrofuran / 3 h / Reflux
With
selenium; Burgess Reagent; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/psc.1276