C₂₀H₃₈O₂Si

Base Information

Chemical Name:C₂₀H₃₈O₂Si
CAS No.:1361965-80-1
Molecular Formula:C₂₀H₃₈O₂Si
Molecular Weight:338.606
Hs Code.:

C<sub>20</sub>H<sub>38</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C₂₀H₃₈O₂Si

Chemical Property:

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Technology Process of C₂₀H₃₈O₂Si

There total 2 articles about C₂₀H₃₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1020192-31-7
C₂₀H₄₄O₂Si₂

: 1361965-80-1
C₂₀H₃₈O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine hydrogenfluoride / tetrahydrofuran / 25.5 h / 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.17 h / 0 °C / Molecular sieve; Inert atmosphere

3.1: tetrahydrofuran / -78 °C

3.2: -78 °C / Heating

With tetrapropylammonium perruthennate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201102630

Reference yield:

: 1361966-02-0
(S)-3-(tert-butyldimethylsilanyloxy)-2,2-dimethylhex-5-en-1-ol⁽¹¹⁾

: 1361965-80-1
C₂₀H₃₈O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.17 h / 0 °C / Molecular sieve; Inert atmosphere

2.1: tetrahydrofuran / -78 °C

2.2: -78 °C / Heating

With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201102630

Reference yield:

: 1361965-80-1
C₂₀H₃₈O₂Si

: 1361965-84-5
C₃₁H₆₀O₃Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / decane; dichloromethane / 0 - 20 °C

2.1: copper(l) cyanide / tetrahydrofuran; diethyl ether / 3.5 h / -55 - -10 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / -78 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -78 °C

4.2: 3 h / -78 °C

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; oxalyl dichloride; bis(acetylacetonate)oxovanadium; copper(l) cyanide; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; decane; dichloromethane; 4.1: Swern oxidation / 4.2: Swern oxidation;
DOI:10.1002/chem.201102630