Technology Process of C62H122O19Si12
There total 4 articles about C62H122O19Si12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; p-toluenesulfonyl chloride;
In
chloroform;
for 1.5h;
Reflux;
DOI:10.1021/ja309558p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Jones reagent / acetone
2: platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane / toluene / 15 °C / Schlenk technique; Inert atmosphere
3: p-toluenesulfonyl chloride; potassium carbonate / chloroform / 1.5 h / Reflux
With
platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane; Jones reagent; potassium carbonate; p-toluenesulfonyl chloride;
In
chloroform; acetone; toluene;
DOI:10.1021/ja309558p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane / toluene / 15 °C / Schlenk technique; Inert atmosphere
2: p-toluenesulfonyl chloride; potassium carbonate / chloroform / 1.5 h / Reflux
With
platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane; potassium carbonate; p-toluenesulfonyl chloride;
In
chloroform; toluene;
DOI:10.1021/ja309558p