C₅₃H₆₅IO₁₃SSi

Base Information

Chemical Name:C₅₃H₆₅IO₁₃SSi
CAS No.:1443651-58-8
Molecular Formula:C₅₃H₆₅IO₁₃SSi
Molecular Weight:1097.15
Hs Code.:

C<sub>53</sub>H<sub>65</sub>IO<sub>13</sub>SSi

Synonyms:

Suppliers and Price of C₅₃H₆₅IO₁₃SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₃H₆₅IO₁₃SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₃H₆₅IO₁₃SSi

There total 13 articles about C₅₃H₆₅IO₁₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1443651-64-6
4-O-acetyl-3-O-tert-butyldimethylsilyl-2-thiophenyl-6-O-tosyl-β-D-glycopyranosyl-(1→4)-α-L-rhodinopyranosyl-(1→4)-2,3-di-O-benzoyl-1-O-benzyl-α-L-rhamnopyranoside

: 1443651-58-8
C₅₃H₆₅IO₁₃SSi

Guidance literature:: With sodium hydrogencarbonate; lithium iodide; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1002/chem.201204545

Reference yield:

: 53270-14-7
benzyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

: 1443651-58-8
C₅₃H₆₅IO₁₃SSi

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 20 °C / Inert atmosphere

2.1: acetic acid / 120 h / 20 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 3 h

5.1: lithium aluminium tetrahydride / 1,4-dioxane / 120 h / Inert atmosphere; Reflux

5.2: Inert atmosphere

6.1: potassium carbonate / methanol / 3 h / Inert atmosphere

7.1: pyridine / dichloromethane / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

9.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -78 °C / Molecular sieve; Inert atmosphere

9.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

10.1: sodium hydrogencarbonate; lithium iodide / tetrahydrofuran / Inert atmosphere; Reflux

With pyridine; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204545

Reference yield:

: 316157-01-4
benzyl 2,3-O-isopropylidene-4-O-(4-methoxybenzyl)-α-L-rhamnopyranoside

: 1443651-58-8
C₅₃H₆₅IO₁₃SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetic acid / 120 h / 20 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 3 h

4.1: lithium aluminium tetrahydride / 1,4-dioxane / 120 h / Inert atmosphere; Reflux

4.2: Inert atmosphere

5.1: potassium carbonate / methanol / 3 h / Inert atmosphere

6.1: pyridine / dichloromethane / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

8.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -78 °C / Molecular sieve; Inert atmosphere

8.2: -78 - 20 °C / Molecular sieve; Inert atmosphere

9.1: sodium hydrogencarbonate; lithium iodide / tetrahydrofuran / Inert atmosphere; Reflux

With pyridine; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1002/chem.201204545