1-(3-TrifluoroMethylphenyl)ethanaMine HCl

Base Information

• Chemical Name: 1-(3-TrifluoroMethylphenyl)ethanaMine HCl
• CAS No.: 3803-25-6
• Molecular Formula: C₉H₁₀F₃N*ClH
• Molecular Weight: 225.641
• Mol file: 3803-25-6.mol

Synonyms:

Chemical Property of 1-(3-TrifluoroMethylphenyl)ethanaMine HCl

Chemical Property:

• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

1-(3-(Trifluoromethyl)phenyl)ethanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-TrifluoroMethylphenyl)ethanaMine HCl

There total 8 articles about 1-(3-TrifluoroMethylphenyl)ethanaMine HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

→ (1R)-1-[3-(trifluoromethyl)phenyl]ethan-1-amine hydrochloride (3803-25-6)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; at 23 ℃; for 1h;

Reference yield: 73.0%

1-(3-(trifluoromethyl)phenyl)ethan-1-iminium chloride → (S)-1-(3-(trifluoromethyl)phenyl)ethan-1-amine hydrochloride (1213939-94-6,3803-25-6)

Guidance literature:

With 2,6-bis(3,5-bis(3,7-bis(trifluoromethyl)naphthalen-1-yl)phenyl)-4H-dinaphtho[2,1-d:1',2'-f][1,3,2]dithiazepine 3,3,5,5-tetraoxide; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate; In tert-butyl methyl ether; methyl cyclohexane; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere; Molecular sieve;

DOI:10.1055/s-0040-1706413

Reference yield:

(S)-1-(3-trifluoromethylphenyl)ethanol (454-91-1,68120-40-1,127852-24-8,96789-80-9) → (1R)-1-[3-(trifluoromethyl)phenyl]ethan-1-amine hydrochloride (3803-25-6)

Guidance literature:

(S)-1-(3-trifluoromethylphenyl)ethanol; With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 40 ℃; for 18h;

With palladium 10% on activated carbon; hydrogen; for 24h; under 7500.75 Torr;

upstream raw materials:

(S)-1-(3-trifluoromethylphenyl)ethanol

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