cyclohex-3-ene-1,1-dicarboxamide

Base Information

• Chemical Name: cyclohex-3-ene-1,1-dicarboxamide
• CAS No.: 640277-10-7
• Molecular Formula: C₈H₁₂N₂O₂
• Molecular Weight: 168.195
• Mol file: 640277-10-7.mol

Synonyms:

Chemical Property of cyclohex-3-ene-1,1-dicarboxamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohex-3-ene-1,1-dicarboxamide

There total 2 articles about cyclohex-3-ene-1,1-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohex-3-ene-1,1-dicarboxylic acid (38511-10-3) → cyclohex-3-ene-1,1-dicarboxamide (640277-10-7)

Guidance literature:

With thionyl chloride; Behandeln des Reaktionsprodukts mit NH 3 in Aether;

DOI:10.1021/ja01163a088

Reference yield:

cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester (38511-09-0) → cyclohex-3-ene-1,1-dicarboxamide (640277-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic KOH

2: SOCl₂ / Behandeln des Reaktionsprodukts mit NH 3 in Aether

With potassium hydroxide; thionyl chloride;

DOI:10.1021/ja01163a088

Reference yield:

cyclohex-3-ene-1,1-dicarboxamide (640277-10-7) → cyclohex-3-ene-1,1-dicarbonitrile (500797-24-0)

Guidance literature:

With phosphoric acid triphenyl ester; phosphorus pentoxide;

DOI:10.1021/ja01163a088

upstream raw materials:

cyclohex-3-ene-1,1-dicarboxylic acid

cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester

Downstream raw materials:

cyclohex-3-ene-1,1-dicarbonitrile