C₆₈H₁₁₀O₁₄Si₂

Base Information

Chemical Name:C₆₈H₁₁₀O₁₄Si₂
CAS No.:143347-83-5
Molecular Formula:C₆₈H₁₁₀O₁₄Si₂
Molecular Weight:1207.78
Hs Code.:

C<sub>68</sub>H<sub>110</sub>O<sub>14</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₈H₁₁₀O₁₄Si₂

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Technology Process of C₆₈H₁₁₀O₁₄Si₂

There total 56 articles about C₆₈H₁₁₀O₁₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123474-67-9
(4R,5S,7R,8S,10R)-7-Benzyloxymethyl-8-methoxy-2,2,10-trimethyl-1,3,6-trioxa-spiro[4.5]decane-4-carboxylic acid ethyl ester

: 143347-83-5,143395-64-6
C₆₈H₁₁₀O₁₄Si₂

Guidance literature:: Multi-step reaction with 11 steps

1: 99 percent / H₂ / Pd(OH)2 / ethanol

2: 1) (COCl)2, DMSO, 2) NEt₃ / 2) CH₂Cl₂, -78 deg C

3: 1) BuLi / 1) THF, -78 deg C

4: Dess-Martin periodinane / CH₂Cl₂

5: 84 percent / Bu₃SnH, AIBN / toluene / Heating

6: 1) CeCl₃*7H₂O, 2) NaBH₄ / 1) MeOH, r.t. to 78 deg C

7: 80 percent / 2,6-di-tert-butylpyridine / CH₂Cl₂

8: 1) OsO₄, NMO, 2) NaIO₄ / 1) THF, H₂O

9: 1a) t-BuLi, 1b) MgBr₂ / 1a) THF, 1b) -78 deg C

10: 78 percent / Dess-Martin periodinane / CH₂Cl₂

11: 1) CeCl₃*7H₂O, 2) NaBH₄ / 1) MeOH, r.t. to 78 deg C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; 2,6-di-tert-butyl-pyridine; cerium(III) chloride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); hydrogen; tert.-butyl lithium; tri-n-butyl-tin hydride; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; magnesium bromide; palladium dihydroxide; In ethanol; dichloromethane; toluene;
DOI:10.1021/jo00045a013

Reference yield:

: 123474-67-9
(4R,5S,7R,8S,10R)-7-Benzyloxymethyl-8-methoxy-2,2,10-trimethyl-1,3,6-trioxa-spiro[4.5]decane-4-carboxylic acid ethyl ester

: 143347-83-5,143395-64-6
C₆₈H₁₁₀O₁₄Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: 99 percent / H₂ / Pd(OH)2 / ethanol

2: 1) (COCl)2, DMSO, 2) NEt₃ / 2) CH₂Cl₂, -78 deg C

3: 1) BuLi / 1) THF, -78 deg C

4: Dess-Martin periodinane / CH₂Cl₂

5: 84 percent / Bu₃SnH, AIBN / toluene / Heating

6: 1) CeCl₃*7H₂O, 2) NaBH₄ / 1) MeOH, r.t. to 78 deg C

7: 80 percent / 2,6-di-tert-butylpyridine / CH₂Cl₂

8: 1) OsO₄, NMO, 2) NaIO₄ / 1) THF, H₂O

9: 1a) t-BuLi, 1b) MgBr₂ / 1a) THF, 1b) -78 deg C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; 2,6-di-tert-butyl-pyridine; cerium(III) chloride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); hydrogen; tert.-butyl lithium; tri-n-butyl-tin hydride; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; magnesium bromide; palladium dihydroxide; In ethanol; dichloromethane; toluene;
DOI:10.1021/jo00045a013

Reference yield:

: 5709-98-8
(R)-cyclohex-3-enecarboxylic acid

: 143347-83-5,143395-64-6
C₆₈H₁₁₀O₁₄Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: 1) MCPBA, 2) Et₃N, SiO₂ / 1) CCl₄, 0 to 25 deg C, 2) 70 deg C

2: 90 percent / imidazole / dimethylformamide / 25 °C

3: NaHCO₃ / 25 °C

4: 2,6-di-tert-butylpyridine / CH₂Cl₂ / 25 °C

5: 100 percent / LiAlH₄ / diethyl ether / 0 °C

6: 1) (COCl)2, DMSO, 2) NEt₃ / 2) CH₂Cl₂, -78 deg C

7: 83 percent / NaH / tetrahydrofuran / -78 °C

8: 1) n-BuLi / 1) THF, -78 deg C

9: 1) Cp₂Zr(H)Cl, 2) N-bromosuccinimide / 1) THF, 40 deg C

10: 1a) t-BuLi, 1b) MgBr₂ / 1a) THF, 1b) -78 deg C

With 1H-imidazole; N-Bromosuccinimide; lithium aluminium tetrahydride; Schwartz's reagent; n-butyllithium; 2,6-di-tert-butyl-pyridine; oxalyl dichloride; tert.-butyl lithium; silica gel; sodium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; magnesium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00045a013