3-(p-bromomethyl)-phenylspiro3,7>decane>

Base Information

Chemical Name:3-(p-bromomethyl)-phenylspiro3,7>decane>
CAS No.:109610-33-5
Molecular Formula:C₁₉H₂₂BrNO
Molecular Weight:360.294
Hs Code.:

3-(p-bromomethyl)-phenylspiro<azetidin-2-one-4,2'-tricyclo<3.3.1.1<sup>3,7</sup>>decane>

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Chemical Property of 3-(p-bromomethyl)-phenylspiro3,7>decane>

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Technology Process of 3-(p-bromomethyl)-phenylspiro3,7>decane>

There total 3 articles about 3-(p-bromomethyl)-phenylspiro3,7>decane> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109610-30-2
1-chlorosulfonyl-3-(p-bromomethylphenyl)spiro3,7>decane>

: 109610-33-5
3-(p-bromomethyl)-phenylspiro3,7>decane>

Guidance literature:: With potassium hydroxide; sodium sulfite; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield:

: 109610-25-5
2-<(4-methylphenyl)methylene>tricyclo<3.3.1.1^3,7>decane

: 109610-33-5
3-(p-bromomethyl)-phenylspiro3,7>decane>

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / NBS, benzoyl peroxide / CCl₄ / 4 h / Heating

2: diethyl ether / a) ice-bath, 8 h, b) RT, 90 h

3: aq. sodium sulfite, aq. KOH / tetrahydrofuran / 2 h / Ambient temperature

With potassium hydroxide; N-Bromosuccinimide; Perbenzoic acid; sodium sulfite; In tetrahydrofuran; tetrachloromethane; diethyl ether;

Reference yield:

: 109610-26-6
2-(p-bromomethyl-phenyl)-methylenetricyclo<3.3.1.1^3,7>decane

: 109610-33-5
3-(p-bromomethyl)-phenylspiro3,7>decane>

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / a) ice-bath, 8 h, b) RT, 90 h

2: aq. sodium sulfite, aq. KOH / tetrahydrofuran / 2 h / Ambient temperature

With potassium hydroxide; sodium sulfite; In tetrahydrofuran; diethyl ether;