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mer-{RhCl3(C6H5CH2CN)3}

Base Information
  • Chemical Name:mer-{RhCl3(C6H5CH2CN)3}
  • CAS No.:42131-07-7
  • Molecular Formula:C24H21Cl3N3Rh
  • Molecular Weight:560.715
  • Hs Code.:
mer-{RhCl<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CN)3}

Synonyms:

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Chemical Property of mer-{RhCl3(C6H5CH2CN)3}
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Technology Process of mer-{RhCl3(C6H5CH2CN)3}

There total 2 articles about mer-{RhCl3(C6H5CH2CN)3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In neat (no solvent); RhCl3(CH3CN)3 dissolved in benzyl cyanide, heated at 100°C for 4h in an open beaker, mixt. cooled to 20-25°C, Et2O added dropwise with continuous stirring; precipitate released, collected on a filter, washed with Et2O, dried inair at room temp., elem. anal., (TLC on SiO2 Rf = 0.69);
DOI:10.1002/(SICI)1099-0682(200006)2000:6<1315::AID-EJIC1315>3.3.CO;2-#
Guidance literature:
With CH(OC2H5)3; warming the educts in the presence of CH(OC2H5)3;
DOI:10.1016/S0020-1693(00)94788-1
Guidance literature:
In toluene; reflux for 1h;
DOI:10.1016/S0020-1693(00)94788-1
upstream raw materials:

phenylacetonitrile

mer-RhCl3(CH3CN)3

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