N,O-diacetyl-2-methylserine methyl ester

Base Information

Chemical Name:N,O-diacetyl-2-methylserine methyl ester
CAS No.:1263775-12-7
Molecular Formula:C₉H₁₅NO₅
Molecular Weight:217.222
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,O-diacetyl-2-methylserine methyl ester

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Technology Process of N,O-diacetyl-2-methylserine methyl ester

There total 1 articles about N,O-diacetyl-2-methylserine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1263775-07-0
(S)-2-methylserine methyl ester (1S)-(+)-camphor-10-sulfonate

: 108-24-7
acetic anhydride

: 1263775-11-6
N-acetyl-2-methylserine methyl ester

: 1263775-12-7
N,O-diacetyl-2-methylserine methyl ester

: 1263775-13-8
N-tert-butoxycarbonyl-O-acetyl-2-methylserine methyl ester

: N,O-di-tert-butoxycarbonyl-2-methylserine methyl ester

: 188476-33-7
(S)-2-N-(tert-butoxycarbonyl)amino-2-methyl-3-hydroxypropanoic acid methyl ester

Guidance literature:: di-tert-butyl dicarbonate; (S)-2-methylserine methyl ester (1S)-(+)-camphor-10-sulfonate; With triethylamine; In tetrahydrofuran; at 4 - 24 ℃; for 20.5h; Inert atmosphere;

acetic anhydride; With triethylamine; In tetrahydrofuran; ethyl acetate; for 0.00833333h; Reflux;
DOI:10.1021/op100299d