C₁₁⁽¹³⁾C₆H₁₄ClNO₃

Base Information

Chemical Name:C₁₁⁽¹³⁾C₆H₁₄ClNO₃
CAS No.:1391745-03-1
Molecular Formula:C₁₇H₁₄ClNO₃
Molecular Weight:321.69
Hs Code.:

C<sub>11</sub><sup>(13)</sup>C<sub>6</sub>H<sub>14</sub>ClNO<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁⁽¹³⁾C₆H₁₄ClNO₃

Chemical Property:

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Technology Process of C₁₁⁽¹³⁾C₆H₁₄ClNO₃

There total 5 articles about C₁₁⁽¹³⁾C₆H₁₄ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391745-01-9
C₈⁽¹³⁾C₆H₁₁ClO₃

: 1391745-03-1
C₁₁⁽¹³⁾C₆H₁₄ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere

3: potassium tert-butylate / 1 h / 20 °C / Inert atmosphere

With oxalyl dichloride; potassium tert-butylate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/jlcr.2924

Reference yield:

: 89059-34-7
[¹³C₆]phenol

: 1391745-03-1
C₁₁⁽¹³⁾C₆H₁₄ClNO₃

Guidance literature:: Multi-step reaction with 5 steps

1: copper; potassium carbonate / tert-butyl methyl ether; dimethyl sulfoxide / 36 h / 130 °C / Inert atmosphere

2: morpholine; sulfur / 24 h / Reflux; Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere

5: potassium tert-butylate / 1 h / 20 °C / Inert atmosphere

With morpholine; oxalyl dichloride; potassium tert-butylate; copper; potassium carbonate; sulfur; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In dichloromethane; tert-butyl methyl ether; dimethyl sulfoxide;
DOI:10.1002/jlcr.2924

Reference yield:

: 1394178-12-1
[⁽¹³⁾C₆]-5-chloro-2-phenoxyacetophenone

: 1391745-03-1
C₁₁⁽¹³⁾C₆H₁₄ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: morpholine; sulfur / 24 h / Reflux; Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere

4: potassium tert-butylate / 1 h / 20 °C / Inert atmosphere

With morpholine; oxalyl dichloride; potassium tert-butylate; sulfur; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/jlcr.2924