Technology Process of C61H74O12Si3
There total 4 articles about C61H74O12Si3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
toluene;
at 20 ℃;
for 48h;
DOI:10.1039/c2sm25763g
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
2: palladium on activated charcoal; hydrogen / tetrahydrofuran / 18 h / 40 °C
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
4: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 48 h / 20 °C
With
dmap; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; palladium on activated charcoal; hydrogen; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2sm25763g
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dicyclohexyl-carbodiimide
2: sodium chlorite
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
4: palladium on activated charcoal; hydrogen / tetrahydrofuran / 18 h / 40 °C
5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C
6: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 48 h / 20 °C
With
dmap; sodium chlorite; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; palladium on activated charcoal; hydrogen; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2sm25763g
