C₄₆H₆₉N₆O₁₂S₃⁽¹⁺⁾

Base Information

• Chemical Name: C₄₆H₆₉N₆O₁₂S₃⁽¹⁺⁾
• CAS No.: 1420991-61-2
• Molecular Formula: C₄₆H₆₉N₆O₁₂S₃
• Molecular Weight: 994.285
• Mol file: 1420991-61-2.mol

Synonyms:

Chemical Property of C₄₆H₆₉N₆O₁₂S₃⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₆H₆₉N₆O₁₂S₃⁽¹⁺⁾

There total 7 articles about C₄₆H₆₉N₆O₁₂S₃⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BrH*C10H25N3O3S + C40H49N4O12S2(1+) → C46H69N6O12S3(1+) (1420991-61-2)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 4 - 20 ℃;

DOI:10.1039/c2ob27190g

Reference yield:

C30H31NO8S (1286282-28-7) → C46H69N6O12S3(1+) (1420991-61-2)

Guidance literature:

Multi-step reaction with 6 steps

1: thionyl chloride / 0.5 h / 85 °C / Inert atmosphere

2: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice; Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 16 h / 95 - 100 °C / Inert atmosphere

4: hydrogenchloride / water / 2 h / Reflux; Inert atmosphere

5: N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 0.25 h / 20 °C

6: sodium hydrogencarbonate / N,N-dimethyl-formamide / 4 - 20 °C

With hydrogenchloride; thionyl chloride; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1039/c2ob27190g

Reference yield:

C30H31ClNO7S(1+) → C46H69N6O12S3(1+) (1420991-61-2)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 1 h / 0 °C / Cooling with ice; Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 16 h / 95 - 100 °C / Inert atmosphere

3: hydrogenchloride / water / 2 h / Reflux; Inert atmosphere

4: N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 0.25 h / 20 °C

5: sodium hydrogencarbonate / N,N-dimethyl-formamide / 4 - 20 °C

With hydrogenchloride; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1039/c2ob27190g

upstream raw materials:

C₃₀H₃₁NO₈S

C₃₄H₄₂N₃O₇S⁽¹⁺⁾

C₃₆H₃₁F₅NO₈S⁽¹⁺⁾

C₃₆H₃₄F₂NO₈S⁽¹⁺⁾

Downstream raw materials:

C₅₅H₇₈N₇O₁₇S₃⁽¹⁺⁾