Technology Process of 1,1-dibutyl-4,5-diphenyl-1,3,2-dioxastannolen
There total 2 articles about 1,1-dibutyl-4,5-diphenyl-1,3,2-dioxastannolen which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
benzene;
byproducts: H2O; benzoin and Bu2SnO refluxing under N2 in benzene under a Dean and Stark trap; benzene distilling off under reduce pressure, red oil treating with pentane, filtering; identified by elem. anal., NMR, Moessbauer spectra;
DOI:10.1016/S0022-328X(00)99502-0
- Guidance literature:
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Di-n-butylcyclopolystannan (1, R: n-Butyl), Benzil, Photolyse;
- Guidance literature:
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In
toluene;
under N2 stannolen in toluene heating under reflux with Bu2SnO; after 10 min oxide dissolving toluene removing under reduce pressure; viscous oil recovering from hexane; identified by elem. anal., IR, Moessbauer spectra;
DOI:10.1016/S0022-328X(00)99502-0
