P(C₆H₅)3WP(OC₆H₅)3(CO)4

Base Information

Chemical Name:P(C₆H₅)3WP(OC₆H₅)3(CO)4
CAS No.:72894-66-7
Molecular Formula:C₄₀H₃₀O₇P₂W
Molecular Weight:868.472
Hs Code.:

P(C<sub>6</sub>H<sub>5</sub>)3WP(OC<sub>6</sub>H<sub>5</sub>)3(CO)4

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P(C₆H₅)3WP(OC₆H₅)3(CO)4

Chemical Property:

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Technology Process of P(C₆H₅)3WP(OC₆H₅)3(CO)4

There total 2 articles about P(C₆H₅)3WP(OC₆H₅)3(CO)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 72894-66-7,72937-35-0
P(C₆H₅)3WP(OC₆H₅)3(CO)4

: 72894-66-7,72937-35-0
P(C₆H₅)3WP(OC₆H₅)3(CO)4

Guidance literature:: In methyl cyclohexane; (N2); soln. of W complex was heated at 80°C for 2 h, cooled to 0°C and seed crystals of cis-isomer were added; after standing overnight at 0°C cis-isomer was filtered off, from mother liquor crystd. trans-isomer on standing at -20°C for 24 h; recrystn. from CH2Cl2/EtOH; elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(00)83486-5

Reference yield: 42.0%

: 101-02-0
triphenyl phosphite

: 18078-18-7,476313-51-6
W(CO)4(P(C₆H₅)3)(NCCH₃)

: 72894-66-7,72937-35-0
P(C₆H₅)3WP(OC₆H₅)3(CO)4

Guidance literature:: In toluene; (N2); soln. of phosphine and W complex was stirred at 20°C for 2 h; filtered soln. was evapd. to dryness and recrystd. from CH2Cl2/EtOH; elem. anal.;
DOI:10.1016/S0022-328X(00)83486-5

Reference yield: 47.0%

: 72894-66-7,72937-35-0
P(C₆H₅)3WP(OC₆H₅)3(CO)4

: 72894-66-7,72937-35-0
P(C₆H₅)3WP(OC₆H₅)3(CO)4

Guidance literature:: In methyl cyclohexane; (N2); soln. of W complex was heated at 80°C for 2 h, cooled to 0°C and seed crystals of cis-isomer were added; after standing overnight at 0°C cis-isomer was filtered off, from mother liquor crystd. trans-isomer on standing at -20°C for 24 h; recrystn. from CH2Cl2/EtOH; elem. anal.; Kinetics;
DOI:10.1016/S0022-328X(00)83486-5