Technology Process of C24H40O5SSi
There total 7 articles about C24H40O5SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 8 h / 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate; dimethylsulfide borane complex / tetrahydrofuran; toluene / 2 h / -10 °C
3.1: di(n-butyl)tin oxide / benzene / 3 h / Reflux
3.2: 0.5 h / 20 °C
4.1: tri-n-butyl-tin hydride; sodium iodide; 1,1'-azobis(1-cyanocyclohexanenitrile) / 1,2-dimethoxyethane / 18 h / 80 °C
5.1: dmap; triethylamine / dichloromethane / 72 h / Reflux
6.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
7.1: calcium chloride / dichloromethane / 18 h / 20 °C
With
dmap; sodium tetrahydroborate; dimethylsulfide borane complex; tri-n-butyl-tin hydride; diisobutylaluminium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; triethylamine; sodium iodide; calcium chloride; 1,1'-azobis(1-cyanocyclohexanenitrile);
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; toluene; benzene;
DOI:10.1055/s-0030-1258327
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 72 h / Reflux
2: diisobutylaluminium hydride / toluene / 2 h / -78 °C
3: calcium chloride / dichloromethane / 18 h / 20 °C
With
dmap; diisobutylaluminium hydride; triethylamine; calcium chloride;
In
dichloromethane; toluene;
DOI:10.1055/s-0030-1258327
