C₅₈H₈₄N₆O₁₁

Base Information

Chemical Name:C₅₈H₈₄N₆O₁₁
CAS No.:1415464-79-7
Molecular Formula:C₅₈H₈₄N₆O₁₁
Molecular Weight:1041.34
Hs Code.:

C<sub>58</sub>H<sub>84</sub>N<sub>6</sub>O<sub>11</sub>

Synonyms:

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Chemical Property of C₅₈H₈₄N₆O₁₁

Chemical Property:

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Technology Process of C₅₈H₈₄N₆O₁₁

There total 10 articles about C₅₈H₈₄N₆O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71460-02-1,173306-82-6
methyl (2S)-2-(tert-butoxycarbonylamino)pent-4-ynoate

: 1415464-79-7
C₅₈H₈₄N₆O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C

1.2: 15 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

3.1: iodine; silver sulfate / methanol

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 15 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

7.1: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 100 °C / Inert atmosphere; Sealed

8.1: trifluoroacetic acid / dichloromethane / 15 °C

9.1: sodium hydrogencarbonate; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 70 °C

With hydrogen; iodine; potassium acetate; sodium hydrogencarbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1415464-72-0
C₁₈H₂₃NO₅

: 1415464-79-7
C₅₈H₈₄N₆O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

2: iodine; silver sulfate / methanol

3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 15 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

6: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 100 °C / Inert atmosphere; Sealed

7: trifluoroacetic acid / dichloromethane / 15 °C

8: sodium hydrogencarbonate; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 70 °C

With hydrogen; iodine; potassium acetate; sodium hydrogencarbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 696-62-8
para-iodoanisole

: 1415464-79-7
C₅₈H₈₄N₆O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C

1.2: 15 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C

3.1: iodine; silver sulfate / methanol

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 0.75 h / 80 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 15 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; acetonitrile / 15 °C

7.1: sodium hydrogencarbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 100 °C / Inert atmosphere; Sealed

8.1: trifluoroacetic acid / dichloromethane / 15 °C

9.1: sodium hydrogencarbonate; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 70 °C

With hydrogen; iodine; potassium acetate; sodium hydrogencarbonate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;