ethyl 4-(cyclohex-2-en-1-yl)butanoate

Base Information

Chemical Name:ethyl 4-(cyclohex-2-en-1-yl)butanoate
CAS No.:120263-81-2
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:

Synonyms:

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Chemical Property of ethyl 4-(cyclohex-2-en-1-yl)butanoate

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Technology Process of ethyl 4-(cyclohex-2-en-1-yl)butanoate

There total 1 articles about ethyl 4-(cyclohex-2-en-1-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 2969-81-5
Ethyl 4-bromobutyrate

: 76644-52-5,76704-31-9,14447-34-8,62247-41-0
rac-3-acetoxycyclohexene

: 120263-81-2
ethyl 4-(cyclohex-2-en-1-yl)butanoate

Guidance literature:: rac-3-acetoxycyclohexene; With manganese; trifluoroacetic acid; cobalt(II) bromide; In acetonitrile; at 20 ℃; for 0.0833333h;

Ethyl 4-bromobutyrate; With pyridine; In acetonitrile; at 80 ℃;
DOI:10.1002/anie.201104390

Reference yield:

: 120263-81-2
ethyl 4-(cyclohex-2-en-1-yl)butanoate

: 120263-83-4
4-Cyclohex-2-enyl-2-diazo-butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na / diethyl ether / 18 h / Ambient temperature

2: 40 percent / Et₃N, 4-toluenesulfonylazide / CH₂Cl₂ / 12 h / Ambient temperature

With 4-toluenesulfonyl azide; sodium; triethylamine; In diethyl ether; dichloromethane;

Reference yield:

: 120263-81-2
ethyl 4-(cyclohex-2-en-1-yl)butanoate

: 120263-86-7
N-(Tricyclo<4.3.0.0^2,9>non-9-yl)carbamidsaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: Na / diethyl ether / 18 h / Ambient temperature

2: 1) Et₃N, tosylazide, 2) Rh(II)-acetate / 1) CH₂Cl₂, 12 h, RT, 2) pentane, 12 h

3: 80 percent / KOH / H₂O; methanol / 8 h / 60 °C

With potassium hydroxide; 4-toluenesulfonyl azide; Rh(II)-acetate; sodium; triethylamine; In methanol; diethyl ether; water;