(methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol

Base Information

• Chemical Name: (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol
• CAS No.: 1204403-25-7
• Molecular Formula: C₁₀₉H₁₃₈N₂O₃₁
• Molecular Weight: 1972.29
• Mol file: 1204403-25-7.mol

Synonyms:

Chemical Property of (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol

There total 1 articles about (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H31NO12S (1151942-33-4) + (2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol (1204403-24-6) → (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol (1204403-25-7) + (methyl 5-acetamido-7,8,9-tri-O-acetyl-5-N,4-O-carbonyl-3,5-dideoxy-D-glycero-β-D-galacto-2-nonulopyranosylonate)-(2->3)-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol

Guidance literature:

C₂₆H₃₁NO₁₂S; (2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol; With N-iodo-succinimide; In dichloromethane; acetonitrile; at -50 ℃; for 0.0833333h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; acetonitrile; at -50 ℃; for 2h; optical yield given as %de; Inert atmosphere;

DOI:10.1002/ejoc.200900778

upstream raw materials:

C₂₆H₃₁NO₁₂S

(2,6-di-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->1)-(2S,3R,E)-3-O-benzoyl-2-octadecanamido-4-octadecene-1,3-diol