Technology Process of C32H42N2O7SSi
There total 6 articles about C32H42N2O7SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane
2: palladium on activated charcoal; hydrogen / methanol
3: pyridine; hydrogen fluoride / tetrahydrofuran
4: di-isopropyl azodicarboxylate / tetrahydrofuran
5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
6: dmap; triethylamine
With
pyridine; dmap; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen fluoride; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
4: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen / methanol
2: pyridine; hydrogen fluoride / tetrahydrofuran
3: di-isopropyl azodicarboxylate / tetrahydrofuran
4: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
5: dmap; triethylamine
With
pyridine; dmap; di-isopropyl azodicarboxylate; palladium on activated charcoal; hydrogen fluoride; hydrogen; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; methanol;
3: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine; hydrogen fluoride / tetrahydrofuran
2: di-isopropyl azodicarboxylate / tetrahydrofuran
3: diisobutylaluminium hydride / tetrahydrofuran / 0 °C
4: dmap; triethylamine
With
pyridine; dmap; di-isopropyl azodicarboxylate; hydrogen fluoride; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran;
2: Mitsunobu reaction;
DOI:10.1073/pnas.1015255108