C₂₇H₃₂Br₄N₂O₆

Base Information

Chemical Name:C₂₇H₃₂Br₄N₂O₆
CAS No.:1452587-24-4
Molecular Formula:C₂₇H₃₂Br₄N₂O₆
Molecular Weight:800.177
Hs Code.:

C<sub>27</sub>H<sub>32</sub>Br<sub>4</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₇H₃₂Br₄N₂O₆

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Technology Process of C₂₇H₃₂Br₄N₂O₆

There total 4 articles about C₂₇H₃₂Br₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1452587-24-4
C₂₇H₃₂Br₄N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium bromochromate / acetic acid / 2 h / 40 °C

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

3: bromine / chloroform / 2 h / 20 °C

4: hydrogen bromide; water / methanol / 48 h

5: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With pyridinium bromochromate; water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 2887-72-1
1-(3,5-dibromo-4-hydroxyphenyl)ethan-1-one

: 1452587-24-4
C₂₇H₃₂Br₄N₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: hydrogen bromide; water / methanol / 48 h

4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 1452587-07-3
C₁₂H₁₃Br₃O₂

: 1452587-24-4
C₂₇H₃₂Br₄N₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / chloroform / 2 h / 20 °C

2: hydrogen bromide; water / methanol / 48 h

3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

With water; hydrogen bromide; bromine; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017