C₆₃H₅₃N₈O₁₈P

Base Information

Chemical Name:C₆₃H₅₃N₈O₁₈P
CAS No.:115264-93-2
Molecular Formula:C₆₃H₅₃N₈O₁₈P
Molecular Weight:1241.13
Hs Code.:

C<sub>63</sub>H<sub>53</sub>N<sub>8</sub>O<sub>18</sub>P

Synonyms:

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Chemical Property of C₆₃H₅₃N₈O₁₈P

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Technology Process of C₆₃H₅₃N₈O₁₈P

There total 5 articles about C₆₃H₅₃N₈O₁₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28288-50-8
N²,O^2',O^3',O^5'-tetrabenzoylguanosine

: 115264-93-2
C₆₃H₅₃N₈O₁₈P

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / sodium methoxide / methanol / 0.07 h / 0 °C

2: 1.) hydrogen chloride / 1.) DMF, R_.T_., 18 h, 2.) 80percent aqueous acetic acid, R_.T_., 2 h.

3: 1.) Dowex 50X₈ (pyridinium form), 2.) 2,4,6-triisopropylbenzenesulfonyl chloride, 1-methylimidazole / 1.) 70percent aqueous pyridine, 0 deg C, 10 min, 2.) acetonitrile, R_.T_.

With 1-methyl-1H-imidazole; hydrogenchloride; 2,4,6-triisopropylphenylsulfonyl chloride; Dowex 50X₈ (pyridinium form); sodium methylate; In methanol;

Reference yield:

: 613-90-1
benzoyl cyanide

: 115264-93-2
C₆₃H₅₃N₈O₁₈P

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / triethylamine / dimethylformamide / 32 h / Ambient temperature

2: 1.) Dowex 50X₈ (pyridinium form), 2.) 2,4,6-triisopropylbenzenesulfonyl chloride, 1-methylimidazole / 1.) 70percent aqueous pyridine, 0 deg C, 10 min, 2.) acetonitrile, R_.T_.

With 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; Dowex 50X₈ (pyridinium form); triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 115265-47-9
C₁₁H₁₇N₃O₈P^(1-)*Li⁽¹⁺⁾

: 115264-93-2
C₆₃H₅₃N₈O₁₈P

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / triethylamine / dimethylformamide / 32 h / Ambient temperature

2: 1.) Dowex 50X₈ (pyridinium form), 2.) 2,4,6-triisopropylbenzenesulfonyl chloride, 1-methylimidazole / 1.) 70percent aqueous pyridine, 0 deg C, 10 min, 2.) acetonitrile, R_.T_.

With 1-methyl-1H-imidazole; 2,4,6-triisopropylphenylsulfonyl chloride; Dowex 50X₈ (pyridinium form); triethylamine; In N,N-dimethyl-formamide;