(1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate)

Base Information

• Chemical Name: (1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate)
• CAS No.: 1134139-10-8
• Molecular Formula: C₂₉H₃₇Cl₂LuO₃
• Molecular Weight: 679.484
• Mol file: 1134139-10-8.mol

Synonyms:

Chemical Property of (1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate)

There total 1 articles about (1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

LuCl3(THF)3 (24614-69-5,144491-06-5,120496-88-0) + sodium 1,3-diphenylcyclopentadienide → (1,3-diphenylcyclopentadienidelutetium dichloride) tris(tetrahydrofuranate) (1134139-10-8)

Guidance literature:

In tetrahydrofuran; byproducts: NaCl; (Schlenk); soln. of LuCl3(C4H8O)3 added with stirring to soln. of ligandin THF, stirred for 24 h; ppt. extd. with THF, concd., residue extd. with toluene, recrystd. from THF; elem. anal.;

DOI:10.1007/s11172-007-0308-5

upstream raw materials:

LuCl₃(THF)3

Refernces