C₁₇H₁₉NO₃Se

Base Information

Chemical Name:C₁₇H₁₉NO₃Se
CAS No.:1268826-62-5
Molecular Formula:C₁₇H₁₉NO₃Se
Molecular Weight:364.303
Hs Code.:

C<sub>17</sub>H<sub>19</sub>NO<sub>3</sub>Se

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₉NO₃Se

Chemical Property:

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Technology Process of C₁₇H₁₉NO₃Se

There total 9 articles about C₁₇H₁₉NO₃Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 736142-03-3
(3aR,10aS,10bS)-octahydro-2H-furo[3,2-c]pyrrolo[1,2-a]azepine-2,8(1H)-dione

: 1268826-62-5
C₁₇H₁₉NO₃Se

Guidance literature:: (3aR,10aS,10bS)-octahydro-2H-furo[3,2-c]pyrrolo[1,2-a]azepine-2,8(1H)-dione; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

Phenylselenyl bromide; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1039/c0ob00850h

Reference yield:

: C₁₃H₁₉NO₄

: 1268826-62-5
C₁₇H₁₉NO₃Se

Guidance literature:: Multi-step reaction with 2 steps

1.1: samarium diiodide; ethanol / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 1 h / -78 °C

With samarium diiodide; ethanol; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1039/c0ob00850h

Reference yield:

: 1268826-56-7
(5S)-{[tert-butyl(dimethyl)silyloxy]methyl}-1-[4-(tetrahydro-2H-pyran-2-yloxy)butyl]pyrrolidin-2-one

: 1268826-62-5
C₁₇H₁₉NO₃Se

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonium fluoride / methanol / 10 h / 20 °C / Reflux

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 - 20 °C

3.1: acetonitrile / 12 h / 20 °C

4.1: toluene-4-sulfonic acid / methanol / 12 h / 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.2: 0.33 h / -78 - 20 °C

6.1: methanol; samarium diiodide / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

7.2: 1 h / -78 °C

With methanol; ammonium fluoride; samarium diiodide; oxalyl dichloride; toluene-4-sulfonic acid; dimethyl sulfoxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 2.1: Swern oxidation / 3.1: Wittig reaction / 5.1: Swern oxidation;
DOI:10.1039/c0ob00850h