C₂₃H₂₇B₁₀NO₃

Base Information

Chemical Name:C₂₃H₂₇B₁₀NO₃
CAS No.:1242177-80-5
Molecular Formula:C₂₃H₂₇B₁₀NO₃
Molecular Weight:473.582
Hs Code.:

C<sub>23</sub>H<sub>27</sub>B<sub>10</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₂₃H₂₇B₁₀NO₃

Chemical Property:

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Technology Process of C₂₃H₂₇B₁₀NO₃

There total 6 articles about C₂₃H₂₇B₁₀NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427079-24-0
C₂₁H₁₆BrNO₃

: 1242177-80-5
C₂₃H₂₇B₁₀NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide; diethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Microwave irradiation

2: potassium carbonate / tetrahydrofuran; methanol / 3 h / 20 °C

3: acetonitrile; toluene / 48 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; diethylamine; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2012.11.081

Reference yield:

: 106-41-2
4-bromo-phenol

: 1242177-80-5
C₂₃H₂₇B₁₀NO₃

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

2: lithium hydroxide; water / tetrahydrofuran / 3 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 8 h / 20 °C

4: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide; diethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Microwave irradiation

5: potassium carbonate / tetrahydrofuran; methanol / 3 h / 20 °C

6: acetonitrile; toluene / 48 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; acetonitrile; 4: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2012.11.081

Reference yield:

: C₂₆H₂₅NO₃Si

: 1242177-80-5
C₂₃H₂₇B₁₀NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; methanol / 3 h / 20 °C

2: acetonitrile; toluene / 48 h / Reflux

With potassium carbonate; In tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.11.081