(Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

Base Information

Chemical Name:(Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate
CAS No.:1427207-81-5
Molecular Formula:C₄₃H₄₆N₄O₁₄S
Molecular Weight:874.923
Hs Code.:

(Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

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Chemical Property of (Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

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Technology Process of (Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

There total 1 articles about (Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-Acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzylcarbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

: 1427207-80-4
(E)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

: 1427207-81-5
(Z)-2-((4aS,5aR,6R,8aS,8bS)-7-((R)-2-acetoxy-1-(4-methoxyphenyl)ethyl)-6-(benzyl(tert-butoxycarbonyl)carbamoyl)-1-((2-nitrophenyl)sulfonyl)-8-oxo-2,4a,5a,6,7,8,8a,8b-octahydro-1H-pyrrolo[3',4':4,5]furo[3,2-b]pyridin-5a-yl)vinyl acetate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Overall yield = 93 %; Overall yield = 1.49 mg; Inert atmosphere;
DOI:10.1021/jm301590z