C₂₁H₁₅BrN₄

Base Information

• Chemical Name: C₂₁H₁₅BrN₄
• CAS No.: 1448517-12-1
• Molecular Formula: C₂₁H₁₅BrN₄
• Molecular Weight: 403.281
• Mol file: 1448517-12-1.mol

Synonyms:

Chemical Property of C₂₁H₁₅BrN₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₁₅BrN₄

There total 1 articles about C₂₁H₁₅BrN₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-bromo-benzaldehyde (1122-91-4) + 2,9-dimethyl-1,10-phenanthroline-5,6-dione (102331-54-4) → C21H15BrN4 (1448517-12-1)

Guidance literature:

With ammonium acetate; In ethanol; for 72h; Inert atmosphere; Reflux;

DOI:10.1039/c3cc44595j

Reference yield: 21.0%

1-bromo-octane (111-83-1) + C21H15BrN4 (1448517-12-1) → C29H31BrN4 (1448517-13-2)

Guidance literature:

C₂₁H₁₅BrN₄; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 40 ℃; Inert atmosphere;

1-bromo-octane; In N,N-dimethyl-formamide; for 68h; Inert atmosphere; Reflux;

DOI:10.1039/c3cc44595j

upstream raw materials:

4-bromo-benzaldehyde

2,9-dimethyl-1,10-phenanthroline-5,6-dione

Downstream raw materials:

C₂₉H₃₁BrN₄