bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid

Base Information

• Chemical Name: bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid
• CAS No.: 861788-34-3
• Molecular Formula: C₁₂H₉AsN₂O₈
• Molecular Weight: 384.134
• Mol file: 861788-34-3.mol

Synonyms:

Chemical Property of bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid

There total 6 articles about bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis-(4-hydroxy-phenyl)-arsinic acid (779354-61-9) → bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid (861788-34-3)

Guidance literature:

With sulfuric acid; nitric acid; at -5 - -3 ℃;

Reference yield:

bis-(4-amino-3-nitro-phenyl)-arsinic acid (872279-15-7) → bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid (861788-34-3)

Guidance literature:

With potassium hydroxide;

Reference yield:

bis-(4-amino-phenyl)-arsinous acid (857587-34-9) → bis-(4-hydroxy-3-nitro-phenyl)-arsinic acid (861788-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Diazotization_.Zersetzung der Diazoverbindung durch Wasserdampf

2: HNO₃+H₂SO₄ / -5 - -3 °C

With sulfuric acid; nitric acid;

upstream raw materials:

bis-(4-amino-3-nitro-phenyl)-arsinic acid

bis-(4-hydroxy-phenyl)-arsinic acid

bis-(4-amino-phenyl)-arsinous acid

Downstream raw materials:

bromo-bis-(4-hydroxy-3-nitro-phenyl)-arsine

chloro-bis-(4-hydroxy-3-nitro-phenyl)-arsine

bis-(3-amino-4-hydroxy-phenyl)-arsinic acid