Technology Process of 5-Decyl-2-(1,4,7,10,13,16,19,22-octaoxa-cyclotetracos-2-ylmethoxy)-benzoic acid methyl ester
There total 8 articles about 5-Decyl-2-(1,4,7,10,13,16,19,22-octaoxa-cyclotetracos-2-ylmethoxy)-benzoic acid methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 67 percent / 1.) AlCl3,CS2 / 1.) reflux, 2 h; 2.) 90-100 deg C, 0.5 h
2: 53 percent / 1.) 15percent aq. NaOH; 2.) 6 N HCl / 20 h / Heating
3: 95 percent / Zn, HgCl2, 6 N HCl / ethanol / 5 h / Heating
4: 51 percent / conc. H2SO4 / Heating; overnight
5: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
hydrogenchloride; carbon disulfide; sodium hydroxide; aluminium trichloride; sulfuric acid; sodium hydride; mercury dichloride; zinc;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / Zn, HgCl2, 6 N HCl / ethanol / 5 h / Heating
2: 51 percent / conc. H2SO4 / Heating; overnight
3: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
hydrogenchloride; sulfuric acid; sodium hydride; mercury dichloride; zinc;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 53 percent / 1.) 15percent aq. NaOH; 2.) 6 N HCl / 20 h / Heating
2: 95 percent / Zn, HgCl2, 6 N HCl / ethanol / 5 h / Heating
3: 51 percent / conc. H2SO4 / Heating; overnight
4: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
hydrogenchloride; sodium hydroxide; sulfuric acid; sodium hydride; mercury dichloride; zinc;
In
ethanol;
