cis-3,5-Dimethylcyclohexanone oxime

Base Information

• Chemical Name: cis-3,5-Dimethylcyclohexanone oxime
• CAS No.: 71364-95-9
• Molecular Formula: C₈H₁₅NO
• Molecular Weight: 141.213
• Mol file: 71364-95-9.mol

Synonyms:

Chemical Property of cis-3,5-Dimethylcyclohexanone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-3,5-Dimethylcyclohexanone oxime

There total 3 articles about cis-3,5-Dimethylcyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3,5-dimethyl-cyclohexanone (7214-52-0) → cis-3,5-Dimethylcyclohexanone oxime (71364-95-9,128925-59-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In methanol; water; at 60 ℃;

DOI:10.1021/jo00128a009

Reference yield:

3,5-dimethyl-cyclohexanone (7214-52-0) → cis-3,5-dimethyl-1-(hydroxyimino)cyclohexane (71364-95-9,128925-59-7)

Guidance literature:

DOI:10.1021/jo01177a006

Reference yield:

3,5-Dimethylphenol (108-68-9,50356-23-5) → cis-3,5-dimethyl-1-(hydroxyimino)cyclohexane (71364-95-9,128925-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: nickel /kieselguhr / 230 °C / 36775.4 Torr / Hydrogenation_.Behandlung der erhaltenen 1.3-Dimethyl-cyclohexanole-⁽⁵⁾ mit CrO₃ in Schwefelsaeure

With kieselguhr; nickel;

upstream raw materials:

3,5-dimethyl-cyclohexanone

3,5-Dimethylphenol

Downstream raw materials:

C₂₀H₂₄NOP

3c,5c-dimethyl-cyclohex-r-ylamine

(+/-)-cis-1.3-dimethyl-cyclohexanone-⁽⁵⁾-(O-benzoyl oxime )

Refernces