Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]-

Base Information

Chemical Name:Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]-
CAS No.:139931-30-9
Molecular Formula:C₁₆H₂₅GeN
Molecular Weight:303.971
Hs Code.:

Synonyms:

Suppliers and Price of Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]-

There total 2 articles about Benzenamine, 2-methyl-N-[3-(triethylgermyl)-2-propynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 16853-85-3
lithium aluminium tetrahydride

: (C₂H₅)3GeCCCHNCH₃C₆H₄

: 139931-30-9
(C₂H₅)3GeCCCH₂NHCH₃C₆H₄

Guidance literature:: With water; In diethyl ether; addn. of a soln. of the Ge compound in abs. ether to a suspension of LiAlH4 in abs. ethers with stirring; stirring for 0.5 h at room temp.;; addn. of H2O; the ppt. was filtered off and washed with ether; the ether extracts were combined and dried over MgSO4; removal of solvent; chromy. (silica gel, ether/hexane (1:3));;

Reference yield: 38.0%

: 16940-66-2
sodium tetrahydroborate

: (C₂H₅)3GeCCCHNCH₃C₆H₄

: 139931-30-9
(C₂H₅)3GeCCCH₂NHCH₃C₆H₄

Guidance literature:: With water; In methanol; addn. of NaBH4 in portions to a soln. of the Ge compound in CH3OH with stirring; stirring for 0.5 h at room temp.;; removal of solvent; addn. of H2O to the residue; extn. with ether; the extracts were dried over MgSO4; removal of solvent; chromy. (silica gel, ether/hexane (1:3));;