O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate
CAS No.:299424-54-7
Molecular Formula:C₆₆H₆₆Cl₃NO₂₄
Molecular Weight:1363.6
Hs Code.:

O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

There total 3 articles about O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 545-06-2
trichloroacetonitrile

: C₆₄H₆₆O₂₄

: 299424-54-7
O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1248/cpb.48.1160

Reference yield:

: C₆₃H₇₂O₂₁Si

: 299424-54-7
O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 317 mg / pyridine / 10 h / 20 °C

2: CF₃COOH / CH₂Cl₂ / 0.5 h / 20 °C

3: 89 mg / DBU / CH₂Cl₂ / 2 h / 0 °C

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In dichloromethane;
DOI:10.1248/cpb.48.1160

Reference yield:

: 299424-53-6
2-(trimethylsilyl)ethyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-β-D-glucopyranoside

: 299424-54-7
O-2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->4)-[(2,3,4-tri-O-acetyl-α-L-fucopyranosyl)-(1->3)]-2-O-benzoyl-6-O-pivaloyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃COOH / CH₂Cl₂ / 0.5 h / 20 °C

2: 89 mg / DBU / CH₂Cl₂ / 2 h / 0 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In dichloromethane;
DOI:10.1248/cpb.48.1160