(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

Base Information

Chemical Name:(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester
CAS No.:1053260-03-9
Molecular Formula:C₆₁H₅₉N₅O₁₂
Molecular Weight:1054.17
Hs Code.:

(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

Synonyms:

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Chemical Property of (S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

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Technology Process of (S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

There total 10 articles about (S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-2-(2-{2-[(S)-2-[3-((S)-3-Benzyloxycarbonyl-2-tert-butoxycarbonylamino-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

: 1053260-03-9
(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1248/cpb.48.308

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 1053260-03-9
(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: WSC*HCl; HOBt; NMM / dimethylformamide

2: TFA / CH₂Cl₂

With 4-methyl-morpholine; WSC*HCl; benzotriazol-1-ol; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.48.308

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 1053260-03-9
(S)-2-(2-{2-[(S)-2-[3-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-benzoylamino]-3-(4-benzyloxy-phenyl)-propionylamino]-phenoxy}-acetylamino)-pentanedioic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: WSC*HCl; HOBt; NMM / dimethylformamide

2: TFA / CH₂Cl₂

3: WSC*HCl; HOBt; NMM / dimethylformamide

4: TFA / CH₂Cl₂

5: WSC*HCl; HOBt; NMM / dimethylformamide

6: TFA / CH₂Cl₂

With 4-methyl-morpholine; WSC*HCl; benzotriazol-1-ol; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.48.308