2-methylphenyllead triacetate

Base Information

• Chemical Name: 2-methylphenyllead triacetate
• CAS No.: 53034-27-8
• Molecular Formula: C₁₃H₁₆O₆Pb
• Molecular Weight: 475.466
• Mol file: 53034-27-8.mol

Synonyms:

Chemical Property of 2-methylphenyllead triacetate

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 2-methylphenyllead triacetate

There total 1 articles about 2-methylphenyllead triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

lead(IV) tetraacetate + bis(2-tolyl) mercury (616-99-9) → 2-methylphenyllead triacetate (53034-27-8)

Guidance literature:

In toluene; addn. of Pb(OAc)4 in toluene to a soln. of Hg-compd. in toluene, stirring at room temp. for 3 days (orange to brown soln.); shaking out the soln. with ethyleneglycol (pale yellow soln.), drying (Na2SO4), filtration, evapn. of filtrate (vac., 50°C), dissoln. of residue in abs. CHCl3, fractional crystn. with petroleum ether (40-60°C) at -30°C; elem. anal.;

DOI:10.1016/0022-328X(92)83382-R

upstream raw materials:

bis(2-tolyl) mercury