CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)={CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)}ClO₄

Base Information

• Chemical Name: CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)={CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)}ClO₄
• CAS No.: 150675-37-9
• Molecular Formula: C₄₄H₃₉AuP₃S*ClO₄
• Molecular Weight: 989.198

Synonyms:

Chemical Property of CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)={CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)}ClO₄

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Useful:

Technology Process of CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)={CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)}ClO₄

There total 1 articles about CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)={CH(P(C₆H₅)2(S))(P(C₆H₅)2(CH₃))(AuP(C₆H₅)3)}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

gold (acetylacetonato) triphenylphosphane + (diphenylphosphinothioyl(methyldiphenylphosphonio)methanide)ClO4 (121578-72-1) → CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)(1+)*ClO4(1-)={CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)}ClO4 (150675-37-9)

Guidance literature:

In dichloromethane; the starting complex is added to the diphosphine in CH2Cl2 at room temp. (ratio complex:ligand 1:1), stirred for 2 h; the soln. is concd., diethyl ether is added, elem. anal.;

DOI:10.1021/om00034a034

Reference yield: 80.0%

CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)(1+)*ClO4(1-)={CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)}ClO4 (150675-37-9) + silver perchlorate → AuAg{CH(P(C6H5)2(S))(P(C6H5)2(CH3))}2(2+)*2ClO4(1-)={AuAg(CH(P(C6H5)2(S))(P(C6H5)2(CH3)))2}(ClO4)2

Guidance literature:

In dichloromethane; AgClO4 is added to the starting phosphine-Au-complex in CH2Cl2; after 2 h the soln. is concd., diethyl ether is added, elem. anal.;

DOI:10.1021/om00034a034

Reference yield:

pentafluorophenyl(tetrahydrothiophene)gold(I) + CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)(1+)*ClO4(1-)={CH(P(C6H5)2(S))(P(C6H5)2(CH3))(AuP(C6H5)3)}ClO4 (150675-37-9) → (bis((diphenylphosphinothioyl(methyldiphenylphosphino)methanide)gold))(ClO4)2

Guidance literature:

In dichloromethane; Au(C6F5)(tht) is added to the starting phosphine-Au-complex in CH2Cl2, stirred for 1 h; the soln. is concd., diethyl ether is added, elem. anal.;

DOI:10.1021/om00034a034

upstream raw materials:

(diphenylphosphinothioyl(methyldiphenylphosphonio)methanide)ClO₄

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