Technology Process of C31H37BrO10
There total 9 articles about C31H37BrO10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanesulfonic acid / 20 °C
2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C
3: sodium acetate; acetic acid / Reflux
With
triethylsilane; methanesulfonic acid; boron trifluoride diethyl etherate; sodium acetate; acetic acid;
In
dichloromethane;
DOI:10.1016/j.cclet.2011.05.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran / -78 °C
1.2: -78 °C
2.1: methanesulfonic acid / 20 °C
3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C
4.1: sodium acetate; acetic acid / Reflux
With
triethylsilane; n-butyllithium; methanesulfonic acid; boron trifluoride diethyl etherate; sodium acetate; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.cclet.2011.05.022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C
2: sodium acetate; acetic acid / Reflux
With
triethylsilane; boron trifluoride diethyl etherate; sodium acetate; acetic acid;
In
dichloromethane;
DOI:10.1016/j.cclet.2011.05.022