(4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane]

Base Information

• Chemical Name: (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane]
• CAS No.: 1415891-58-5
• Molecular Formula: C₃₆H₅₈O₅Si₃
• Molecular Weight: 655.11

Synonyms:

Chemical Property of (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane]

Chemical Property:

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MSDS Files:

Useful:

Technology Process of (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane]

There total 1 articles about (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

C36H58O5Si3 (1415891-32-5) → (4aR,6S,10aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)hexahydro[1,3,2]dioxasilino[5,4-b]oxocin-7(6H)-one (1415891-33-6) + (4aR,6R,10aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)hexahydro[1,3,2]dioxasilino[5,4-b]oxocin-8(9H)-one (1415891-34-7) + (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane] (1415891-35-8) + (4aR,6S,9aS)-2,2-di-tert-butyl-6-(((tert-butyldiphenylsilyl)-oxy)methyl)-3'-(trimethylsilyl)hexahydrospiro[[1,3,2]dioxasilino[5,4-b]oxepino-7,2'-oxirane] (1415891-58-5)

Guidance literature:

With pyridinium p-toluenesulfonate; In methanol; dichloromethane; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo302267f

upstream raw materials:

C₃₆H₅₈O₅Si₃

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