Cyclopenta[c]pyrrole-2(1H)-carboxylic acid, hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2- yl)oxy]methyl]-, methyl ester

Base Information

Chemical Name:Cyclopenta[c]pyrrole-2(1H)-carboxylic acid, hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2- yl)oxy]methyl]-, methyl ester
CAS No.:139936-63-3
Molecular Formula:C₂₃H₃₁NO₆
Molecular Weight:417.502
Hs Code.:

Cyclopenta[c]pyrrole-2(1H)-carboxylic acid,
hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2-
yl)oxy]methyl]-, methyl ester

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Chemical Property of Cyclopenta[c]pyrrole-2(1H)-carboxylic acid, hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2- yl)oxy]methyl]-, methyl ester

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Technology Process of Cyclopenta[c]pyrrole-2(1H)-carboxylic acid, hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2- yl)oxy]methyl]-, methyl ester

There total 5 articles about Cyclopenta[c]pyrrole-2(1H)-carboxylic acid, hexahydro-5-oxo-1-[(phenylmethoxy)methyl]-4-[[(tetrahydro-2H-pyran-2- yl)oxy]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139936-62-2
(S)-1-Benzyloxymethyl-5-oxo-4-(tetrahydro-pyran-2-yloxymethyl)-3,3a,4,5-tetrahydro-1H-cyclopenta[c]pyrrole-2-carboxylic acid methyl ester

: 139936-63-3
(S)-1-Benzyloxymethyl-5-oxo-4-(tetrahydro-pyran-2-yloxymethyl)-hexahydro-cyclopenta[c]pyrrole-2-carboxylic acid methyl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃;
DOI:10.1039/c39920000169

Reference yield:

: 139936-59-7
(S)-1-Benzyloxymethyl-prop-2-ynylamine

: 139936-63-3
(S)-1-Benzyloxymethyl-5-oxo-4-(tetrahydro-pyran-2-yloxymethyl)-hexahydro-cyclopenta[c]pyrrole-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0 - 20 °C

2: NaH / dimethylformamide / 0 - 20 °C

3: 2.) N-methylmorpholine N-oxide (NMO) / 1.) benzene, RT, 2.) CH₂Cl₂, 0 deg C

4: LiAlH₄, CuI, hexamethylphosphoric triamide (HMPA) / tetrahydrofuran / -78 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium aluminium tetrahydride; sodium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39920000169

Reference yield:

: 139936-60-0
((S)-1-Benzyloxymethyl-prop-2-ynyl)-carbamic acid methyl ester

: 139936-63-3
(S)-1-Benzyloxymethyl-5-oxo-4-(tetrahydro-pyran-2-yloxymethyl)-hexahydro-cyclopenta[c]pyrrole-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 0 - 20 °C

2: 2.) N-methylmorpholine N-oxide (NMO) / 1.) benzene, RT, 2.) CH₂Cl₂, 0 deg C

3: LiAlH₄, CuI, hexamethylphosphoric triamide (HMPA) / tetrahydrofuran / -78 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium aluminium tetrahydride; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c39920000169